Industrial Policy and the International Economy by Albert Fishlow, Jean Carrière, Sueo Sekiguchi

By Albert Fishlow, Jean Carrière, Sueo Sekiguchi

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1989). , 1987) in mixtures of up to 7%. Unfortunately, the lifetime of the bead is shortened with polar modifiers in the fluid. 36 SUPERCRITICAL FLUIDS IN INDUSTRIAL ANALYSIS Heating the bead in a flame was found in early work to result in low sensitivity in SFC. Recently, however, Mol et al. (1991) showed that by adjusting the hydrogen flow, the air flow and the bead position, very promising results were obtained in phosphorus-selective determination of pesticides. With packed capillary columns and modifiers added to carbon dioxide, the minimum detectable quantity was 15-65 pg of pesticides.

J. , 295, 315-322. , Tanaka, M. , (1989), Purged splitless injection in microcolumn SFC. J. Chromatogr. , 27, 395-398. , Koshiba, H. , (1990), Introduction of large sample volumes in capillary SFC. J. High Resolut. , 13, 619-623. , Kadota, Y. , (1991), Technique for injecting very large volumes in capillary SFC. J. Microcol. , 3, 17-25. Hoffmann, S. , (1989), Packed capillary SFC with mixed mobile phases and light-scattering detection. J. Microcol. , 1, 35-40. Huang, E. E. , (1988), Direct heated interface probe for capillary SFC/double focusing MS.

With detectors like the FID, the detector temperature is usually set to approximately 350 °C. The actual temperature of the fluid is not known, but much lower. With detectors where the temperature affects important properties of the aerosol coming from the restrictor, such as the light-scattering detector, heating of the restrictor must be fine-tuned. For the majority of detectors this is not the case. 2. 7 Detectors SFC incorporates elements from GC as well as from HPLC, including the detectors.

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